Metrohm 796 Titroprocessor User Manual

Page 140

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8.2 DET

796 Titroprocessor, Instructions for use

134

134

Titration conditions

These are the actual titration parameters that control the dosing procedure
and recording of measured values during the titration.

Adjustment

Pre-defined sets of parameters

slow | medium | fast

To facilitate setting the titration parameters, there is a
choice of three different sets of parameters. These sets
comprise a number of tried-and-tested settings which will
suffice for the vast majority of requirements.

slow

for ultra-precise titrations or for chemically
inhibited reactions requiring a long time

medium

standard parameter for non-problematical
titrations, optimized for the most common
applications

fast

fastest pre-set parameter for non-critical
titrations

If the titration parameters need to be modified to specific ti-
tration problems, the various pre-set parameters can be
adjusted on an individual basis.
The softkey [Custom adjust] opens another dialogue
window in which user-defined settings can be entered (see
p. 137f).

Temperature

Setting the temperature or its measuring mode

-170…25.0…500°C | auto | initial

The temperature during a titration can be determined
automatically using a Pt100/Pt1000 sensor or a combined
electrode with integral temperature sensor and can (with
measuring quantity pH) be used to correct the pH auto-
matically. The temperature during a titration can be re-
corded and printed out as a temperature curve.

numerical

Manual input (e. g. to correct the pH)

auto

Automatic measurement throughout the
entire titration (for temperature curve)

initial

Single measurement at the beginning
of the titration mode

The temperature can be integrated in formulas for calcula-
tions (see p. 129), e. g. for volume corrections. The follow-
ing system variables are generated:

IT

Initial temperature at start of mode

ST

Start temperature before first dosing
(

auto only)

CT

End temperature at last dosing
(

auto only)

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