Metrohm 796 Titroprocessor User Manual

Page 177

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8. Command reference

796 Titroprocessor, Instructions for use

171

171

A value up to 150 mL/min can also be entered for smaller
buret cylinders; however, when the method is carried out
the dosing speed will automatically be reduced to the larg-
est possible value. For KF reagents (viscous liquids) no
filling rate greater than 30 mL/min should be selected as
otherwise too rapid filling may cause a partial vacuum in
the cylinder (bubble formation!).

Temperature

Temperature setting or measuring mode

-170…25.0…500°C | auto | initial

The temperature can be automatically determined during a
titration with the aid of a Pt100/Pt1000 sensor or a com-
bined electrode with built-in temperature sensor. It is pos-
sible to record the temperature throughout a titration and to
output it as a temperature curve.

numerical

manual input

auto

automatic measurement during the
whole titration (for temperature curve)

initial

one-off measurement at the start of the
titration mode

The temperature can be included in formulas for calcula-
tions (see page 119ff), e.g. for volume corrections. The dif-
ferent system variables are listed on page 149 and 129.
Please note: Start temperature ST and closing tempera-
ture

CT are only available with auto.

U(pol)

Polarization voltage (with KFC_UPOL*)

-1270…400…1270 mV

The polarization voltage is the voltage which is applied to a
polarized electrode during amperometric titration. The re-
sultant measuring quantity is I

pol

/µA.

I(pol)

Polarization current (with KFC_IPOL*)

-127…25…127 µA

The polarization current is the current which is applied to a
polarized electrode during voltametric titration. The resul-
tant measuring quantity is U

pol

/mV.

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