Metrohm 796 Titroprocessor User Manual

Page 172

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8.6 KFT

796 Titroprocessor, Instructions for use

166

166

Min. increment

Smallest possible volume step

0.1…9.99 µL | min

In order to avoid excessively slow titration speeds (and
thus "never-ending" waiting times) during dynamically
controlled titrations the smallest possible volume incre-
ment can be set. This parameter should only be altered
with caution, as too large volume increments can nega-
tively influence the accuracy of the results.

Max. rate

Largest possible titration speed

0.01…150 mL/min | max

Setting the max. rate has a direct effect on the dosing
speed of the titration control. The maximal value depends
on the cylinder size of the buret.

Buret cylinder

max. speed

1 mL

3 mL/min

2 mL

6 mL/min

5 mL

15 mL/min

10 mL

30 mL/min

20 mL

60 mL/min

50 mL

150 mL/min

A value up to 150 mL/min can also be entered for smaller
buret cylinders; however, when the method is carried out
the dosing speed will automatically be reduced to the larg-
est possible value.

Stop crit

.

Switch-off mode

drift | time | none

The stop criterion defines the behavior of the titrator
when the endpoint is reached. The automatic termina-
tion of the titration can be carried out according to dif-
ferent criteria:

Drift

The titration is stopped when (after the EP
has been reached) the volume drift falls
below the set value.

Time

After the EP has been reached the set time
is allowed to elapse before the titration is
stopped.

none

The titration will not be stopped automati-
cally. The sample solution will be kept at
the endpoint.

If a renewed addition is necessary before the stop crite-
rion is recognized then a further volume increment will
be added and the stop criterion again checked.

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