INFICON 3000 Micro GC Gas Analyzer Operating Manual User Manual

Page 15

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TOC - 7

PN

07

4-

51

9-

P1

C

3000 Micro GC Operating Manual

Chapter 8

Instrument Operations

8.1

Routine Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-1

8.1.1

System Bakeout . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-1

8.1.2

Shutdown/Restart . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-3

8.1.3

Standby . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-4

8.2

Remove and Replace a 3000 Micro GC Module . . . . . . . . . . . . . . . . . . . . . 8-5

8.2.1

Types of Replacement Modules . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-5

8.2.2

Performance Enhanced GC Module vs. Standard GC Module . . . . . . . . . . 8-5

8.2.3

Update the Instrument Firmware . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-6

8.2.4

Decommission a Standard GC Module . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-7

8.2.5

Remove a GC Module . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-11

8.2.6

Install a GC Module . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-16

8.2.7

Commission a New Standard GC Module . . . . . . . . . . . . . . . . . . . . . . . . . 8-20

8.2.8

Enable the Instrument in EZ IQ . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-22

8.3

Sample Conditioners . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-23

8.3.1

Sample Conditioner Connections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-23

8.3.1.1

Connections for Sample Inlet Filter (PN G2801-60900),
Pressure Reducer (PN G2815A),
Pressure Reducer and Genie Filter Assembly (PN G2816A), and
Genie Filter Assembly (PN G2817A) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-23

8.3.1.2

Connections for the Heated Regulator
(PN G2818A-X/G2845A-X/G2857A-X). . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-23

8.3.1.3

Connections for the Heated Vaporizer
(PN G2819A-X/G2846A-X/G2858A-X). . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-23

8.3.2

Running a Low Pressure, Clean Gas Sample . . . . . . . . . . . . . . . . . . . . . . 8-24

8.3.3

Running a Low Pressure, Liquid/Particulate Containing Gas Sample . . . . 8-25

8.3.4

Running a High Pressure Gas Sample without Liquids/Particulates . . . . . 8-26

8.3.5

Running a High Pressure Gas Sample with Liquids/Particulates . . . . . . . . 8-27

8.3.6

Running a High Pressure Gas Sample Containing C6+ Components . . . . 8-28

8.3.6.1

Using a Sample Vessel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-28

8.3.6.2

Using a Transfer Line or Other Continuous Sample Source . . . . . . . . . . . 8-30

8.3.7

Running a High Pressure Liquid Petroleum Gas Sample. . . . . . . . . . . . . . 8-32

8.4

Consumable Replacement Procedures . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-35

8.4.1

Replacing the External 10 Micron Sample Inlet Filter Disk. . . . . . . . . . . . . 8-35

8.4.2

Replacing the 2 Micron Filter in the Heated Vaporizer
(PN G2819A-X/G2846A-X/G2858A-X). . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-36

8.4.3

Replacing the 7 Micron Filter in the Heated Regulator
(PN G2818A-X/G2845A/G2857A) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-37

8.5

Portable 3000 Micro GC Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-38

8.5.1

General Information and Cautions of the Portable 3000 Micro GC . . . . . . 8-38

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