Titration sequence for kft – Metrohm 840 PC Control 5.0 / Touch Control User Manual

Page 227

Advertising
background image

4

Parameters

PC Control / Touch Control

215

adapted to the size of the titration cell in order to prevent any over-

flow.

Cond. stop time: If conditioning takes longer than the time entered

here then the process will be stopped.

Start reconditioning only at end of method: If this option is

switched on then reconditioning will only start when all method

commands have been processed. Otherwise reconditioning would

start immediately after the titration command. This function must be

activated if other commands follow the KFT command that must not

be allowed to take place at the same time as conditioning. Exam-

ple: emptying the titration cell and then adding new solution.

The parameters for Control device, Sensor, Dosing device and

Stirrer

are described in Section 4.1.5.

Titration sequence for KFT

1st start of titration

command

Checks whether work is to be carried out with or

without conditioning.

(Switch on stirrer)

The stirrer is switched on after the start.

Preconditioning

(if activated)

The titration cell solution is titrated to the end-

point and kept there continuously.

2nd start of titration

command

The method sequence itself starts.

Measure initial meas-

ured value

The initial measured value is measured.

(Start conditions:

Pause 1

Start volume

Pause 2)

Pause interval 1 is allowed to elapse. The start

volume is added. No measuring points are en-

tered in the list of measuring points. Pause inter-

val 2 is allowed to elapse.

(Extraction time)

Titration with test up

to stop when stop

criterion or the stop

condition is reached

Titration is carried out.

If the extraction time has not elapsed when the

endpoint has been reached then it will be al-

lowed to elapse and the titration will only be

concluded when the extraction time has

elapsed.

(Switch off stirrer)

The stirrer is switched off if there is no recondi-

tioning.

Fill dosing

cylinder

After the end of the titration the dosing cylinder is

refilled automatically.

Post-conditioning

The titration cell solution is kept continuously at

the endpoint.

Optional steps are shown in brackets.

Advertising