4) calibration and validation, A) manual calibration – Yokogawa GC8000 Process Gas Chromatograph User Manual

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<1. Overview>

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IM 11B08A01-01E

● In the case where a pause command is received during the run mode in the stream

specifi cation status [2H2]

The operation mode is immediately prepared to be changed to the pause mode in the

stream specifi cation status.

The operation mode changes to the pause mode in the stream specifi cation status at a

preset time during the measurement of the currently-measured stream.

The pause command can be canceled with a cancel command until the operation mode

changes to the pause mode.

● In the case where a run command is received during the pause mode in the stream

specifi cation status [2G6]

The suspended measurement is resumed.

Run

Run

Pause

Rest of W1

Rest of S1

W1

W1

W1

S1

S1

S1

W1

S1

W1

W1

S1

Time

Stream sequence 1

Run command

[2H2]

[2G6]

Pause command

(4) Calibration and validation

Three types of calibration and validation methods are available as follows.

Manual

Selection of a calibration (or validation) number, switching of stream valves to fl ow the

standard sample, and issue of a calibration (or validation) start command are all performed

manually.

Semiautomatic

Once a calibration (or validation) number is selected, stream valves are automatically

switched to fl ow the standard sample, then calibration (or validation) starts automatically.

Automatic

Stream valves are automatically switched to fl ow the standard sample, then calibration (or

validation) starts automatically at a preset date, time, and interval. The preset calibration (or

validation) patterns of which automatic execution is enabled are automatically executed.

The details of these three types of calibration and validation are described below.

(a) Manual calibration

To select the calibration (or validation) method, touch the “Calibration (validation) method”
button to open the selection window on the GCM operation status screen on the GC-HMI
analyzer operation display (Figure 1.23) or select it on the “Calibration/validation setting”
screen on the EtherLCD (Figure 1.24). A set of stream numbers and the numbers of times
of measurement is specifi ed for each of Calibration 1 to 6 and Validation 1 to 6 on the
“Calibration/validation setting” screen on the EtherLCD. Users at Level C or higher are
allowed to select the calibration (or validation) method.

Next, issue a command to change the measurement status to a preset status among
Calibration 1 to 6 or Validation 1 to 6 on the calibration (validation) window on the GCM
operation status screen. Calibration (or validation) numbers for which stream numbers are
not specifi ed are not in the options. If there is no calibration (or validation) numbers for which
stream numbers are specifi ed, the operation button is invalid and is displayed in gray.

Select a calibration (or validation) number, and then touch the “OK” button. Then the
waiting measurement status is changed to the selected calibration (or validation) number
on the overall GCM information screen. Users at Level B or higher are allowed to select the
calibration (or validation) number.

Users at Level C or higher can cancel the command to change the measurement status
to the specifi ed calibration (or validation) status until the waiting measurement status is
changed to the selected calibration (or validation) number and the measurement of the
currently-measured stream is completed.

2nd Edition : May 11, 2012-00

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